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LI Quan, YANG Xiao-mei, CHENG Xiao-hong, ZHAO Yuan-hong. A simple synthesis of "Queen substance"[J]. Journal of Yunnan University: Natural Sciences Edition, 2008, 30(6): 611-613.
Citation: LI Quan, YANG Xiao-mei, CHENG Xiao-hong, ZHAO Yuan-hong. A simple synthesis of "Queen substance"[J]. Journal of Yunnan University: Natural Sciences Edition, 2008, 30(6): 611-613.
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A simple synthesis of "Queen substance"

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  • A simple synthesis of "Queen substance"(trans-9-Oxo-dec-2enoic acid)was reported.Monobromination of 1,6-hexandiol followed by protection with 3,4-dihydro-2H-pyran afforded compound 2.After addition between Grignard reagent of compound 2 and acetaldehyde,deprotection and oxidation by pyridinium chlorochromate(PCC),a Kaoevenagle reaction finally provided the "Queen Substance" in 25.55% overall yield.
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