殷彩霞, 高竹林, 黄荣. 大环化合物八甲基环二十碳四烯八酮的合成[J]. 云南大学学报(自然科学版), 2003, 25(1): 48-49,52.
引用本文: 殷彩霞, 高竹林, 黄荣. 大环化合物八甲基环二十碳四烯八酮的合成[J]. 云南大学学报(自然科学版), 2003, 25(1): 48-49,52.
shu
YIN Cai-xia, GAO Zhu-lin, HUANG Rong. Synthesis of a macrocyclic compound-octamethylcy cloeicosatetraeneoctaketone[J]. Journal of Yunnan University: Natural Sciences Edition, 2003, 25(1): 48-49,52.
Citation: YIN Cai-xia, GAO Zhu-lin, HUANG Rong. Synthesis of a macrocyclic compound-octamethylcy cloeicosatetraeneoctaketone[J]. Journal of Yunnan University: Natural Sciences Edition, 2003, 25(1): 48-49,52.
shu

大环化合物八甲基环二十碳四烯八酮的合成

Synthesis of a macrocyclic compound-octamethylcy cloeicosatetraeneoctaketone

    摘要
  • 摘要: 通过呋喃和丙酮在酸性溶液中的缩合,得到大环化合物八甲基四氧杂口夸哒烯(1),化合物(1)经间氯过氧苯甲酸氧化,得八甲基环二十碳四烯八酮(2).化合物(1)和(2)的结构均经IR,1HNMR,13CNMR,MS得到验证.

     

    Abstract: A macrocyclic compound,octamethylcycloeicosatetraeneoctaketone,was synthesized through two step reactions.Firstly,octamethyltetroxaquaterene (1) was obtained by condensation of furan and acetone.Octamethylcycloeicosatetraeneoctaketone (2) was synthesized by oxidation of compound(1)using m-chloroperoxybenzic acid.Compound(1)and compound(2) were identified by analysis of spectral data of IR,MS, 1HNMR,13CMNR.

     

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