杨薇, 唐长明, 李显, 周娅, 王丽, 李良. 毛杨梅化学成分的研究[J]. 云南大学学报(自然科学版), 2011, 33(4): 453-457 .
引用本文: 杨薇, 唐长明, 李显, 周娅, 王丽, 李良. 毛杨梅化学成分的研究[J]. 云南大学学报(自然科学版), 2011, 33(4): 453-457 .
Study on the chemical constituents of Myrica esculenta[J]. Journal of Yunnan University: Natural Sciences Edition, 2011, 33(4): 453-457 .
Citation: Study on the chemical constituents of Myrica esculenta[J]. Journal of Yunnan University: Natural Sciences Edition, 2011, 33(4): 453-457 .

毛杨梅化学成分的研究

Study on the chemical constituents of Myrica esculenta

  • 摘要: 对产于云南西双版纳的毛杨梅的化学成分进行研究,采用硅胶柱层析、重结晶等分离手段从中分离纯化得到13个化合物,通过现代波谱技术和理化常数测定鉴定了它们的结构,分别为:myricitrin(1),myricanol(2),myricanone(3),没食子酸(gallic acid,4),ethyl β-D-glucopyranoside(5),间羟基苯甲醛(3-hydroxybenzaldehyde,6),异香草醛(7),对甲氧基苯甲酸(4-methoxybenzoic acid,8),对羟基苯甲醇(4-(hydroxymethyl)phenol,9),β-扶桑甾醇(β-rosasterol,10),β-谷甾醇(β-sitosterol,11),胡萝卜苷(daucosterol,12).首次用X-单晶衍射验证了化合物2的结构.

     

    Abstract: The chemical constituents of Myrica esculenta were studied and thirteen compounds were isolated by the method of silica gel column chromatography and recrystallization.Their structures were elucidated as myricitrin(1),myricanol(2),myricanone(3),gallic acid(4),ethyl β-D-glucopyranoside(5),3-hydroxybenzaldehyde(6),isovanillin(7),4-methoxybenzoic acid(8),4-(hydroxymethyl)phenol(9),β-rosasterol,(10),β-sitosterol (11),daucosterol (12) by spectral data analysis and comparison with the reported data and standard samples.The structure of compound 2 was also confirmed by X-ray diffraction for the first time.

     

/

返回文章
返回